Core-interlayer-shell Fe3O4/SiO2/TiO2, CoFe2O4/SiO2/TiO2 and BaFe12O19/SiO2/TiO2 magnetic photocatalysts were obtained. A water-in-oil microemulsion system with suitable surfactants was used for functionalization of the magnetic core with silica interlayer and TiO2-based photocatalyst. Uncoated and coated particles were characterized by electrophoretic meaurements, X-ray diffractometry (XRD), scanning electron microscopy (SEM), transmision electron microscopy (TEM), specific surface area (BET) measurements, diffuse reflectance spectroscopy (DRS) and vibrating sample magnetometer (VSM) analysis. The pH of the solution and corresponding zeta potential was found to be essential for appropriate formation of ferrite core/silica layer/TiO2 shell nanocomposite, since the electrical charge controls interactions during functionalization of the magnetic core particles.
Authors
- prof. dr hab. inż. Anna Zielińska-Jurek link open in new tab ,
- mgr inż. Zuzanna Bielan link open in new tab ,
- dr inż. Szymon Dudziak link open in new tab ,
- Izabela Malinowska link open in new tab ,
- Zuzanna Sobczak link open in new tab ,
- prof. dr hab. inż. Tomasz Klimczuk link open in new tab ,
- Grzegorz Nowaczyk,
- prof. dr hab. inż. Jan Hupka link open in new tab
Additional information
- DOI
- Digital Object Identifier link open in new tab 10.3390/catal7120360
- Category
- Publikacja w czasopiśmie
- Type
- artykuł w czasopiśmie wyróżnionym w JCR
- Language
- angielski
- Publication year
- 2017