Graphene hydrogels were prepared by ascorbic acid-assisted gelation of graphene oxide (GO) aqueous suspensions both in acidic and basic conditions. Different mass ratio of ascorbic acid (AA) to GO was used (namely 20:1 and 10:1). In order to eliminate the influence of AA on the final structure of hydrogels, samples without AA were prepared by a hydrothermal gelation of GO in an autoclave. An in-depth structural characterization of the obtained materials was performed before and after supercritical drying by means of FTIR, XRD and SEM. Surface area of hydrogels was determined using the methylene blue adsorption method. BET surface area and pore volume analysis of aerogels was also performed. The effect of initial GO concentration and volume on the final graphene aerogels structure was determined. Electrochemical properties of samples were also evaluated. Finally, gold nanoparticles (Au NP) adsorption on graphene hydro- and aerogels was presented for the first time. Graphene hydrogels and aerogels are promising candidates for practical applications e.g. in the Au NP removal from wastewater.
Autorzy
- mgr inż. Izabela Kondratowicz link otwiera się w nowej karcie ,
- dr hab. inż. Kamila Sadowska link otwiera się w nowej karcie ,
- Małgorzata Nadolska link otwiera się w nowej karcie ,
- dr inż. Agata Jażdżewska link otwiera się w nowej karcie ,
- prof. dr hab. inż. Maria Gazda link otwiera się w nowej karcie
Informacje dodatkowe
- DOI
- Cyfrowy identyfikator dokumentu elektronicznego link otwiera się w nowej karcie 10.1016/j.colsurfa.2017.05.063
- Kategoria
- Publikacja w czasopiśmie
- Typ
- artykuł w czasopiśmie wyróżnionym w JCR
- Język
- angielski
- Rok wydania
- 2017