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Publications from the year 2024
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Continuous Biomedical Monitoring in VR Scenarios of Socially Smart and Safe Autonomous Vehicle Interaction
- Tomasz Kocejko
- Abdeljalil Abbas-turki
- Alexandre Brunoud
Pedestrians, as vulnerable road users, pose safety challenges for autonomous vehicles (AVs). Their behavior, often unpredictable and subject to change, complicates AV-pedestrian interactions. To address this uncertainty, AV s can enhance safety by communicating their planned trajectories to pedestrians. In this research, we explore the interaction between pedestrians and autonomous vehicles within an industrial environment, focusing on how communicative behavior from the vehicles influences pedestrians' physiology. We investigate the possibility of mea-suring biosignals while participants wear a VR headset and experiment a pedestrian crossing. Our preliminary study reveals subtle variations in delta rhythms when users immersed in VR simulations interact with AV s that either provide or withhold additional information.
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Continuum contact model for friction between graphene sheets that accounts for surface anisotropy and curvature
- Aningi Mokhalingam
- Shakti Gupta
- Roger Sauer
Understanding the interaction mechanics between graphene layers and co-axial carbon nanotubes (CNTs) is essential for modeling graphene and CNT-based nanoelectromechanical systems. This work proposes a new continuum contact model to study interlayer interactions between curved graphene sheets. The continuum model is calibrated and validated using molecular dynamics (MD) simulations. These are carried out employing the reactive empirical bond order (REBO)+Lennard-Jones (LJ) potential to model the interactions within a sheet, while the LJ, Kolmogorov-Crespi (KC), and Lebedeva potentials are used to model the interactions between sheets. The continuum contact model is formulated for separation distances greater than 0.29 nm, when sliding contact becomes non-dissipative and can be described by a potential. In this regime, sheet deformations are sufficiently small and do not affect the sheet interactions substantially. This allows to treat the master contact surface as rigid, thus simplifying the contact formulation greatly. The model calibration is conducted systematically for a sequence of different stackings using existing and newly proposed ansatz functions. The calibrated continuum model is then implemented in a curvilinear finite element (FE) shell formulation to investigate the pull-out and twisting interactions between co-axial CNTs. The resisting pull-out forces and torques depend strongly on the chirality of the considered CNTs. The absolute differences between FE and MD results are very small, and can be attributed to model assumptions and loading conditions.
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Controlled engineering of Bi4O5Br2 and BiOBr via interactions imidazolium ionic liquids and medium during synthesis as a simple method for enhancement of photocatalytic activity
- Aleksandra Bielicka-giełdoń
- Patrycja Wilczewska
- Rafał Ślusarz
- Artur P. Terzyk
- Patrycja Parnicka
- Karol Szczodrowski
- Jacek Ryl
- Fei Qi
- Ewa Siedlecka
Ionic liquid-mediated synthesis of Bi4O5Br2 and BiOBr was carried out in non-polar solvents (glycerol, ethylene glycol) and a polar solvent (0.1 M mannitol). The effect of elongation of alkyl side chains (C4mim+, C8mim+, and C16mim+) of imidazolium ionic liquids, which act as a source of bromide and template, on the morphological, optical, and photocatalytic properties of materials was investigated. The crystallite size, morphology, particle size, energy bandgap, and exposure of (110), (001), and (102) facets were effectively tuned by selecting the proper ionic liquid–solvent system. The self-assembly of ILs and their role in forming Bi-based crystallites in non-polar and polar solvents differed. The most effective 5-fluorouracil was photooxidized over the samples prepared in C4mim+ – 0.1 M mannitol solution, while the best Cr(VI) photoreduction occurred with the sample formed in C4mim+ – glycerol. Molecular dynamics simulation correlated the length of alkyl side chains of imidazolium ILs with an increase in the number of “free” –OH groups of the solvent, which interacted with BiOBr nuclei during synthesis, fine-tuning its photocatalytic activity.
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Controlling nodal displacement of pantographic structures using matrix condensation and interior-point optimization: A numerical and experimental study
- Ahmed Manguri
- Najmadeen Saeed
- Robert Jankowski
This study presents an innovative approach for the precise control of nodal displacements in pantographic structures. The method is founded on the Matrix Condensation of Force Method, seamlessly integrated with an Interior Point Optimization algorithm. This combination offers a unique advantage by allowing users to manipulate displaced nodes within a defined coordination domain. Furthermore, this approach introduces the Interior Point Optimization algorithm as an indispensable tool to eliminate inactive turnbuckles and minimize overall actuation requirements. Traditional control methods typically demand a substantial number of turnbuckles and extensive actuation efforts to attain the desired nodal coordinates. The interconnected nature of node movements, wherein changes in one node affect others, adds complexity to determining the impact of bar length alterations on each node. To address this challenge, precisely control power of the Interior Point Optimization algorithm systematically explores numerous scenarios to identify solutions that minimize both actuation and turnbuckle usage. The current technique's effectiveness is validated through rigorous comparisons with established methods, experimental modeling, and rigorous testing using SAP 2000 software. Notably, the current approach yields remarkable results, requiring a staggering 60% less actuation and reducing the reliance on turnbuckles by up to 40% compared to previous methods. This innovation promises to significantly enhance the efficiency and cost-effectiveness of controlling pantographic structures, marking a substantial advancement in this field.
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Controlling the europium oxidation state in diopside through flux concentration
- N. Górecka
- Tadeusz Lesniewski
- Sebastian Mahlik
- Marcin Łapiński
- Y.-T. Tsai
- Aleksandra Bielicka-giełdoń
- Karol Szczodrowski
This paper explores the connection between the H3BO3 flux concentration and the co-existence of Eu2+ and Eu3+ dopants within CaMgSi2O6 crystals (diopside). The samples were synthesised using a solid-state synthesis method under varying atmospheric conditions, including oxidative (air), neutral (N2), and reductive (H2/N2 mixture) environments. Additionally, some materials underwent chemical modification by partially substituting Si4+ with Al3+ ions acting as charge compensation defects stabilizing Eu3+ luminescence. Depending on the specific synthesis conditions, the materials predominantly displayed either the orange-red luminescence of Eu3+ (under oxidising conditions) or the blue luminescence of Eu2+; however, the comprehensive results confirmed the co-existence of Eu3+/Eu2+ luminescence in both cases. This work shows that varying flux concentrations added during synthesis significantly affect the relative strength of Eu2+ and Eu3+ emissions in a manner dependent on the synthesis atmosphere. The emission of Eu2+ increases with a higher flux concentration in materials synthesised under oxidative and neutral atmospheres independent of the chemical modification. In contrast, for materials obtained under a reductive atmosphere, the changes in the Eu3+ emission intensity depended on the presence or absence of Al3+ ions namely the increase of flux increased the Eu3+ intensity in the case of unmodified materials and decreased in the Al-modified ones. All observed effects were qualitatively explained considering the double role of the flux in the studied system, which besides facilitating the diffusion of chemical species during synthesis acts as a charge compensating agent by creating B′Si centres stabilizing Eu3+ emission.
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Convenient and efficient N-methylation of secondary amines under solvent-free ball milling conditions
- Mikołaj Walter
- Olga Ciupak
- Karol Biernacki
- Janusz Rachoń
- Dariusz Witt
- Sebastian Demkowicz
In the present work, we report the development of a rapid, efcient, and solvent-free procedure for the N-methylation of secondary amines under mechanochemical conditions. After optimization of the milling parameters, a vibrational ball mill was used to synthesize 26 tertiary N-methylated amine derivatives in a short time of 20 min (30 Hz frequency) and high yields ranging from 78 to 95%. An exception was compounds having a hydroxyl group in their structure, for which a decrease in reaction efciency was observed. During our research, we investigated alternate reaction selectivity occurring in compounds able to form ring closure products that are 3,4-dihydro-2H-1,3-benzoxazine derivatives instead of N-methylated products. The liquid-assisted grinding technique has been applied using formalin as a methylating agent and sodium triacetoxyborohydride as a reducing agent in a reductive amination reaction.
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Corncob-supported calcium oxide nanoparticles from hen eggshells for cadmium (Cd-II) removal from aqueous solutions; Synthesis and characterization
- Werkne Sorsa Muleta
- Sultan Mulisa Denboba
- Abreham Bayu
This study investigated the efficient removal of cadmium ions from aqueous solutions using calcium oxide nanoparticles (CaO NPs) synthesized from waste hen eggshells using a Sol-gel method and supported on corncob bio-adsorbent. The synthesized CaO NPs were characterized using FT-IR, XRD, specific surface area, and TGA. Batch adsorption experiments were conducted to examine the influence of process parameters such as adsorbent dosages, initial Cd (II) concentrations, pH values, and contact times. XRD analysis revealed that the synthesized CaO nanoparticles had a size of 24.34 nm and a specific surface area of 77.4 m2 g. The optimal conditions for achieving the highest percent removal of cadmium (99.108%) were found to be an initial concentration of 55 ppm, pH 7, adsorbent dose of 0.75 g, and contact time of 50 min. The experimental removal efficiency closely matched the predicted value (99.0%), indicating the suitability of the method used in optimizing the removal of Cd (II) ions from aqueous solutions. These findings, corroborated by predicted values, underscore the efficacy of our method in optimizing cadmium removal. Based on these findings, it can be concluded that corncob-supported CaO NPs are optimized for their highest efficiency and hold great promise as a cost-effective and environmentally friendly solution for wastewater treatment with a focus on cadmium removal.
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Corporate social responsibility and forward default risk under firm and industry heterogeneity
- Muhammad Mushafiq
- Błażej Prusak
- Magdalena Markiewicz
Objective: This study aims to evaluate the impact of corporate social responsibility on forward default risk (FDR) under the setting of firm and industry heterogeneity. Research Design & Methods: This study evaluated the impact of corporate social responsibility (CSR) on FDR using the data of 497 companies from 2007-2021 in the S&P 500 index, taking into account firm and industry heterogeneity aspects. This study utilized instrumental variable regression using the generalized method of moments (IV-GMM) estimation technique which is robust for controlling the pertinent issue of endogeneity. Findings: This study found a negative relationship between CSR and FDR in the full sample. From the firm size aspect, this study found that CSR is more effective in mitigating FDR in large-cap firms than in mid-cap firms. Firm age heterogeneity exhibited a distinct behaviour, as young and middle-aged firms had a stronger impact on FDR management in comparison to old firms. Industry heterogeneity showed that industries with higher customer interaction have a higher impact on corporate social responsibility to control FDR. Industries with lower customer interaction have a lower impact on corporate social responsibility and FDR. Implications & Recommendations: We proposed some policy recommendations based on the findings in the context of firm and industry heterogeneity. Especially the management of mid-cap and young corporations should improve the CSR policy to enhance CSR performance which would lead to stabilized protection against FDR. Similarly, consumer-intensive industries should also focus on enhancing CSR initiatives to decrease FDR. Non-consumer-intensive industries should focus on enhancing CSR policy and at the same time pay particular attention to communicating CSR results to end consumers to reduce FDR. Contribution & Value Added: This study is the first to explore CSR’s impact on financial parameters under heterogeneity.
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Correlations of structural, thermal and electrical properties of sodium doped complex borophosphosilicate glass
- Zuzanna Milewczyk
- Sharafat Ali
- Piotr Okoczuk
- Jacek Ryl
- Ryszard Barczyński
- Natalia Wójcik
Borophosphosilicate glasses with varying sodium ion concentrations were investigated for their, structural, thermal, and electrical properties. All the obtained glasses were transparent except the glass with the highest sodium content, which exhibited translucency due to inhomogeneities. Increasing sodium content led to reduced boron and silicon content while maintaining a constant B/Si ratio, indicating progressive depolymerization of the glass network. Confocal microscopy, scanning electron microscopy, and atomic force microscopy showed homogeneous and granular structure for samples with lower sodium content, but higher sodium content resulted in visible agglomeration/nanocrystallization. X-ray diffractograms showed amorphous nature for most samples, with samples doped with the highest concentrations of Na2O showing several broad reflections suggesting nanoscale crystallinity. Fourier-transform infrared spectroscopy revealed shifts in dominant bands with increasing sodium content, indicating depolymerization of the borate network. An observed decrease in glass transition temperature and thermal stability with increasing sodium content was attributed to depolymerization and formation of non-bridging oxygens. Impedance spectroscopy revealed two relaxation processes associated with the transport of Na+ ions through two different regions. DC conductivity and activation energy predominantly increased with the sodium ion content at high temperatures.
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Corrigendum to “An investigation on residual stress and fatigue life assessment of T-shape welded joints” [Eng. Fail. Anal. 141 (2022) 106685]
- Jeetendra Mourya
- Greg Wheatley
- Mohammed Nizam Khan
- Reza Masoudi Nejad
- Ricardo Branco
- Wojciech Macek
This paper aims to quantitatively evaluate the residual stress and fatigue life of T-type welded joints with a multi-pass weld in different direction. The main research objectives of the experimental test were to test the residual stress by changing direction along with multiple wielding passes and determine the fatigue life of the welded joints. The result shows that compressive residual stress increases in the sample gradually from single-pass weld to double and triple-pass weld. Moreover, the fatigue life of the specimen also gradually improves with an increasing number of welding passes. Performing multi-pass welding in different directions affects the material’s residual stress and fatigue life, which is an essential factor to consider for assuring the strength of the welded joint.
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Corrigendum to “Experimental analysis on the risk of vortex ventilation and the free surface ventilation of marine propellers”
- Anna Kozłowska
The paper presents a discussion of the ventilation inception and air drawing prediction of ships propellers, aiming to predict under what conditions ventilation will happen, and the actual physical mechanism of the ventilation.
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Corrigendum to “Fatigue life improvement using low transformation temperature weld material with measurement of residual stress” [Int. J. Fatigue 164 (2022) 107137]
- Jordan Franks
- Greg Wheatley
- Pedram Zamani
- Reza Masoudi Nejad
- Wojciech Macek
- Ricardo Branco
Welding processes often produce high levels of tensile residual stress. Low transformation temperature (LTT) welding wires utilise phase transformation strains to overcome the thermal contraction of a cooling weld. In this paper, the residual stress within each weld was quantified using the milling/strain gauge method, being the strain change measured as the weldment was milled away. The fatigue tests were conducted under uniaxial loading considering two types of LTT materials. The results show that the crack propagation of all samples was similar in cycles although both LTT materials extended the crack initiation, and, therefore, the overall life of the part. It was found that both LTT materials reduced the residual tensile stresses, increased the residual compressive stresses, leading to increase in fatigue life about 30%.
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Corrigendum to “The influence of α,ω-diols and SiO2 particles on CO2 absorption and NH3 escaping during carbon dioxide capture in ammonia solutions” [J. CO2 Util. 80 (2024) 102698]
- Temesgen Amibo
- Donata Konopacka-Łyskawa
nie dotyczy
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Corrosion damage identification based on the symmetry of propagating wavefield measured by a circular array of piezoelectric transducers: Theoretical, experimental and numerical studies
- Beata Zima
- Jochen Moll
The article investigates the results obtained from numerical simulations and experimental tests concerning the propagation of guided waves in corroded steel plates. Developing innovative methodologies for assessing corrosion-induced degradation is crucial for accurately diagnosing offshore and ship structures exposed to harsh environmental conditions. The main aim of the research is to analyze how surface irregularities affect wave propagation characteristics. An investigation was conducted for antisymmetric fundamental mode A0. Specifically, the study examines the asymmetrical wavefronts generated by nonuniform thickness in damaged specimens. Initially, numerical analysis explores the impact of thickness variation on wave field symmetry. Corroded plates with varying levels of degradation are modeled using the random fields approach, with degradation levels ranging from 0 % to 60 %. Subsequently, the research investigates how the standard deviation of thickness distribution (from 5 % to 20 % of the initial thickness) and excitation frequency (from 50 to 150 kHz) influence recorded signals and the shape of reconstructed wavefronts. Each scenario compares wavefront symmetry levels estimated using rotational and bilateral symmetry degrees as indicative parameters. The numerical simulations are complemented by experimental tests conducted on plates with three different degradation levels. The results demonstrate the efficacy of the proposed wave field analysis approach for assessing structural integrity, as evidenced by the agreement between numerical predictions and experimental observations.
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Corrosion Inhibition of AZ31-xLi (x = 4, 8, 12) magnesium alloys in sodium chloride solutions by aqueous molybdate
- Maria Osipenko
- Andrei Paspelau
- Aliaksandr Kasach
- Jacek Ryl
- Konrad Skowron
- Janusz Adamiec
- Irina Kurilo
- Dmitry Kharitonov
Corrosion of lithium-containing AZ31 magnesium alloys AZ31-xLi (x = 4, 8, and 12 wt%) has been examined in 0.05 M NaCl solution with and without 10–150 mM of Na2MoO4 inhibitor. Potentiodynamic polarization, electrochemical impedance spectroscopy (EIS), and dynamic electrochemical impedance spectroscopy (DEIS) measurements were used to correlate the phase composition and microstructure of the alloys with their corrosion propensity and effectiveness of the molybdate inhibitor, giving high inhibition efficiency (>85%) at concentrations higher than ca. 35 mM. Post-corrosion microstructure, Raman, and X-ray photoelectron spectroscopy analyses allowed to provide the inhibition mechanism of AZ31-xLi alloys by molybdate ions.
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Corrosion Monitoring in Petroleum Installations—Practical Analysis of the Methods
- Juliusz Orlikowski
- Agata Jazdzewska
- Iwona Łuksa
- Michał Szociński
- Kazimierz Darowicki
This paper presents the most typical corrosion mechanisms occurring in the petroleum industry. The methods of corrosion monitoring are described for particular corrosion mechanisms. The field and scope of the application of given corrosion-monitoring methods are provided in detail. The main advantages and disadvantages of particular methods are highlighted. Measurement difficulties and obstacles are identified and widely discussed based on actual results. Presented information will allow the corrosion personnel in refineries to extract more reliable data from corrosion-monitoring systems.
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Corrosion of AISI1018 and AISI304 steel exposed to sulfates
- Ginneth Millan Ramirez
- Miguel Angel Baltazar-Zamora
- Ce Tochtli Méndez Ramírez
- Maciej Niedostatkiewicz
- Hubert Byliński
This research analyses the behavior of corrosion, durability, and quality of reinforced concrete samples coated with two different materials when exposed to contaminated soil with sulfates. The initial assessment involved evaluating the water absorption rate of the coating materials before and after exposure to a solution containing 3%푁푎2푆푂4+3%푀푔푆푂4+3%퐾2푆푂4+3%퐶푎푆푂4to determine their durability. the corrosion potential and linear polarization resistance technique were employed to measure the corrosion rate. Carbon steel and AISI 304 steel bars were tested alongside a stainless counter electrode. The findings indicate that the solvent-based coating exhibited superior performance, demonstrating reduced corrosion and water absorption rates. Additionally, the presence of sulfates led to the formation of a surface layer on the concrete, initially aiding in limiting waterpenetration. However, over time, this layer eventually causes damage to the concrete from the inside out.
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Corrosion performance of super duplex stainless steel and pipeline steel dissimilar welded joints: a comprehensive investigation for marine structures
- Anup Kumar Maurya
- Shailesh M. Pandey
- Rahul Chhibber
- Dariusz Fydrych
- Chandan Pandey
This study investigates the corrosion behavior of dissimilar gas tungsten arc (GTA) welded joints between super duplex stainless steel (sDSS 2507) and pipeline steel (X-70) using electrochemical and immersion corrosion tests. The GTA welds were fabricated using ER2594 and ER309L fller metals. The study examined the electrochemical characteristics and continuous corrosion behavior of samples extracted from various zones of the weldments in a 3.5 wt.% NaCl solution, employing electrochemical impedance spectroscopy, potentiodynamic polarization methods, and an immersion corrosion test. EIS and immersion investigations revealed pitting corrosion in the X-70 base metal/X-70 heat-afected zone, indicating inferior overall corrosion resistance due to galvanic coupling. The corrosion byproducts identifed in complete immersion comprised α-FeOOH, γ-FeOOH, Fe3O4, and Fe2O3, whereas γ-FeOOH and Fe3O4 were predominant in dry/wet cyclic conditions. Corrosion escalated with dry/wet cycle conditions while maintaining a lower level in complete immersion. The corrosion mechanism involves three wet surface stages in dry/wet cycles and typical oxygen absorption during complete immersion. Proposed corrosion models highlight the infuence of Cl−, O2, and rust layers.
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Cost-effective methods of fabricating thin rare-earth element layers on SOC interconnects based on low-chromium ferritic stainless steel and exposed to air, humidified air or humidified hydrogen atmospheres
- Łukasz Mazur
- Paweł Winiarski
- Bartosz Kamecki
- Justyna Ignaczak
- Sebastian Molin
- Tomasz Brylewski
Most oxidation studies involving interconnects are conducted in air under isothermal conditions, but during real-life solid oxide cell (SOC) operation, cells are also exposed a mixture of hydrogen and water vapor. For this study, an Fe–16Cr low-chromium ferritic stainless steel was coated with different reactive element oxides – Gd2O3, CeO2, Ce0.9Y0.1O2 – using an array of methods: dip coating, electrodeposition and spray pyrolysis. The samples underwent oxidation experiments carried out over 100 h in three different atmospheres at 800 °C: air, an air/H2O mixture, and an Ar/H2/H2O mixture. The influence of different atmospheres on the corrosion of the Fe–16Cr steel was determined via oxidation kinetics studies; the corrosion product was evaluated using X-ray diffraction, scanning electron microscopy and area-specific resistance (ASR) measurements. All coated samples exhibited lower parabolic oxidation rate constants than bare steel and most also had lower ASR. The applied modifications were found to be sufficiently effective to allow the investigated low-chromium steel to be considered for application as an interconnect material for SOCs.
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Cost-Effective Piggyback Forward dc-dc Converter
- Oleksandr Matiushkin
- Oleksandr Husev
- Hossein Afshari
- Dmitri Vinnikov
- Ryszard Strzelecki
The novel piggyback dc-dc converter as a cost-effective solution is presented in this work. It provides a wide input voltage range of regulation with a low component count. The novel solution is an advanced forward dc-dc converter with an additional clamp output capacitor. The idea of such a type of converter is to transfer magnetizing energy of transformer to the output side, instead of using input clamp circuit. The design guidelines of the passive component of the proposed solution are discussed. A digital domain proportional integral controller is designed for the off-grid system validation, and it provides a stable output voltage in a wide range of the input voltage and power. Experimental prototype of the proposed piggyback converter along with experimental results of critical points are presented. The efficiency study of the proposed solution is done.